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双语推荐:晶体质量

压电晶体传感器利用压电石英晶体振荡频率对晶体表面质量负载和表面性状的高度敏感性,来实现对物质微质量的检测。介绍了压电晶体传感器的原理,给出了检测系统的硬件组成及数据处理与分析软件设计,分析了其应用现状,并对该检测系统的发展趋势进行了展望。
The piezoelectric crystal sensors used the characteristic that the oscillation frequency of the piezoelectric crystal is highly sensitive to the load and properties on crystal surface, such as density, viscosity, conductivity and dielectric constant to carry out materials micro-quality test. Introduction was made to the principle of the piezoelectric crystal sensors. This paper designed the hardware composition, data processing and analysis software of the detection system and analyzed the system’s application actuality, looking forward to the development trend of the detection system.

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采用垂直沉积法组装了二元聚苯乙烯胶粒晶体,研究了两种聚苯乙烯胶体微球的粒径比、质量比、温度和分散介质中乙二醇含量等因素对二元聚苯乙烯胶粒晶体组装花样的影响.粒径比4.45、质量比≥74∶26是形成面心立方二元聚苯乙烯胶粒晶体的必要条件.组装温度为60℃,分散介质中乙二醇质量分数为6%时,可得到更高质量的二元聚苯乙烯胶体晶体.胶体微球二元垂直沉积机理研究表明:两种聚苯乙烯胶体微球是同时在基片的表面进行组装的;胶体微球在介质中的布朗运动、沉降速率及其在基片表面的组装速率三者之间匹配越好,所得二元聚苯乙烯胶粒晶体质量越高.
Binary colloidal crystals were fabricated by a vertical deposition method with two sub-micrometer size polystyrene ( PS) microspheres. The self-assembled patterns of binary colloidal crystals ( bCCs) were investigated by varying the size ratio, the mass ratio of PS microspheres, the temperature and content of ethylene glycol in water. It is found that PS binary colloidal crystals with face-cen-tered cube (fcc) arrangement can be obtained while the size ratio is more than 4. 45 and the mass ratio is not less that 74:26. High-quality PS binary colloidal crystals are easily generated at the temperature of 60℃ and the mass fraction of ethylene glycol in dispersing medium of 6%. The study also shows that self-assembly of two PS microspheres on the substrate surface is operated at the same time, and in this regard the vertical deposition method has a great deal of difference from other methods. In addition, PS binary colloidal crystals have a higher quality with the increase of ma

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单晶硅的氧含量及其均匀性可显著影响各种硅基器件的性能,也是在硅晶体生长过程中较难控制的参数。本文分析了直拉单晶硅生产过程中氧杂质的引入机理及其对晶体质量的影响,并通过改变氩气流量或炉内压力、热场几何尺寸、埚位、晶体转速和坩埚转速等拉晶条件,以及采用相应的磁拉技术来控制晶体中的氧含量及分布均匀性,提高晶体质量
The oxygen content and its uniformity of single silicon crystal will significantly affect the performance of all kinds of silicon-based apparatus.The parameters of the oxygen content and the uniformity are difficult to be controlled dur-ing silicon crystal growth process.This paper analyzed the mechanism of the introduction of oxygen impurities in czochralski single crystal silicon and the impacts on the quality of the crystal.It can control the crystal oxygen content and distribution uniformity to improve crystal quality by controlling pulling conditions such as changing argon gas flow or furnace pressure, changing thermal field geometry,changing crucible position or changing the crystal and the crucible rotation speed and tak-ing the appropriate magnetic field pulling technologies,so the quality of that was improved.

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碲锌镉晶体中存在着各种典型晶体缺陷,x射线衍射形貌术是一种非破坏性地整体研究晶体材料结构完整性、均匀性的有效方法。本文将反射式x射线衍射形貌术应用于碲锌镉晶体质量的评价,研究了入射线狭缝宽度、积分时间、扫描步长等测试参数以及样品表面加工状态对x射线衍射形貌的影响。结果表明入射线狭缝宽度对碲锌镉晶体的x射线衍射成像及晶体质量筛选应用影响很大,积分时间、样品扫描步长等测试参数的选择与入射线狭缝宽度密切相关。
Many kinds of typical crystal defects can be observed in the Cadmium Zinc Telluride (CdZnTe)single crystals. X-ray diffraction topography is a powerful method for the investigation of structural integrity and homogeneity of single crystals. In this paper,reflection X-ray diffraction topography is applied to evaluate the quality of CdZnTe single crystals. The effect of the factors of incident beam slit,exposure time,scanning step and surface roughness on the X-ray diffraction topography are studied. Results show that the incident beam slit is the most important factor to the X-ray diffraction topography of defects,which is also closely related to the application of screening substrates by crystal quality. The parameters of exposure time and scanning step are closely related to the incident beam slit.

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在多焦点人工晶体实际使用中,影响其成像质量的因素主要有:瞳孔直径、后房深度以及由此引起的偏心、倾斜等。本文通过ZEMAX软件在Liou&Brennan眼模型基础上进行改进,用ReZoom多焦点人工晶体替代眼模型原有晶体,建立多焦点人T晶体眼模型,模拟上述影响因素的变化,计算不同条件下MTF传递函数并进行比较分析,归纳出各因素对于成像质量的影响。主要结果如下:多焦点人r品体植人人眼后,后房深度、瞳孑L直径、倾斜和偏心对成像质量均有影响。对于后房深度7.8mm,瞳孔直径2mm左右的患者,成像质量最佳,随着瞳孔直径和后房深度的增加,成像质量逐渐下降;另外,如果出现晶体的倾斜和偏心,都会引起成像质量的下降,在倾斜范围3。以内,对成像效果的影响不大。
In the use of MIOL (Multifocal Intraocular Lens), there are three main influencing factors of imaging quality, which are the pupil diameter, posterior chamber depth, and the related eccentricity and tilt. This paper uses the ZEMAX to establish a MIOL eye model by replacing Liou&Brennan eye model’s former lens with ReZoom MIOL, simulate changes in factors, calculate the MTF, dissertates the four factors in theory and analyzes the degree of inlfuence. The main results are as follows:after the MIOL implantation in the human eye, the posterior chamber depth, pupil diameter, tilt and eccentricity all have inlfuence on the imaging quality. The patient who has pupil diameter of 2 mm and posterior chamber depth of 7.8 mm has the best image quality. As the pupil diameter and posterior chamber depth increases, the image quality decreased. In addition, lens tilt and eccentricity will cause a decline in image quality, but less than 3 degrees tilt has little effect on the imaging results.

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为了研究钾钠铌酸锶钡KNSBN晶体的全息存储特性,设计了相关实验结构,通过改变物光与参考光在KNSBN晶体中形成的体相位栅的位置,研究了体相位栅在晶体内不同位置对体全息再现像质量的影响及再现时的衍射效率.研究结果表明:当体相位栅到晶体前端的距离为2.0~3.5mm时,再现图像质量相对稳定;当距离 L=3.0mm时衍射效率达到最大值31%,此时再现像保持时间最长,可达到262 s;图像质量最好,亮度大,稳定性好且再现像不失真.实验结果证实了KNSBN 晶体可作为一种优良的体全息存储介质,且在体全息存储中,尽可能的将物光与参考光叠加形成的体相位栅置于晶体内部时,再现时将能得到较高的衍射效率和质量较高的再现图像.
The self‐designed experiment system was established to research the holographic storage properties of potassium sodium strontium barium niobate crystal-KNSBN .The different position of the volume grating in the crystal ,which affected the quality of reproduced image and diffraction efficiency of reproduction ,was studied by changing the position of object light and reference light in crystal KNSBN . The reproduced image quality was best and the reconstructed image kept a longest time and relatively stable ,when the distance between volume phase grating and the front of crystal was in the range of 2 .0~3 .5 mm ,especially the diffraction efficiency was 31% when the distance L= 3 .0 mm .This time produced image duration was longest ,262 seconds ,image quality was best ,luminance was biggest , stability was best and produced image did not distortion .The experimental results confirmed that the crystal KNSBN could be used as an excellent volume holographic storage media ,and it

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为了提出测定果糖质量分数的新方案,采用光子晶体平面波展开法进行了理论分析和数值模拟。通过研究以硅半导体材料为背景介质周期性排列空气孔圆柱构成的光子晶体,分别取得了正方晶格和三角晶格的空气孔结构光子晶体的TE模、TM模禁带结构特性。结果表明,在高频率区域,2维正方晶格或三角晶格结构各向同性光子晶体的光子带隙随待测质量分数不同是单调变化的;同时,晶格结构对光子带隙有一定的影响,不论是在正方结构还是三角结构光子晶体中,TE模带隙都比TM模大得多。这对质量分数测量和高血糖患者的临床应用有一定的指导作用。
In order to propose a novel method to measure the mass fraction of fructose,plane wave expansion method for photonic crystal was adopted.A 2-D photonic crystal with a square lattice and triangle lattice of circular cylinders was designed in the Si background semiconductor material.The TE mode and TM mode band gap structure characteristics of square lattice and triangular lattice air hole structure photonic crystal were achieved.The results show that for isotropic photonic crystal of either square or triangular array arrangement,it is easier for the dielectric air type photonic crystal to form TE-polarized mode band gap in high-frequency region.Lattice structure has a certain impact on photonic band gap, TE mode band gap is much larger than the TMmode in both square and triangular structure photonic crystal.The photonic band gap changes with the difference of the mass fraction of the fructose solutions,which are used as the dielectric material in the air hole.

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分别在基片水平、倾斜和垂直3种不同条件下采用784 nm SiO2微球自组装制备胶体光子晶体。研究了3种不同条件下制备胶体晶体的区别以及各自的优、缺点,对垂直条件下制备样品进行光学性能的表征,简单分析了自组装过程中胶体晶体的成形机理。结果表明:对于微球粒径较大的SiO2胶体晶体的制备,水平条件下适用于制备二维胶体晶体,倾斜和垂直条件下可以获得面积较大、质量较高的三维胶体晶体
Three different self-assembly methods,including level,oblique and vertical evaporation were used to prepare colloidal photonic crystals with 784 nm SiO2 microspheres. The differences,advantages and disadvantages of colloidal crystals under three preparation conditions were compared,optical properties of the sample prepared under vertical condition were characterized, and the forming mechanism of the self-assembly process of colloidal crystals was analyzed. The results show that for the preparation of larger microsphere size SiO2 colloidal crystals,the level conditions are suitable for the preparation of two-dimensional colloidal crystals,and oblique and vertical conditions can prepare larger,high-quality three-dimensional colloidal crystals.

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研究了铁钛共掺蓝宝石(Fe, Ti:Sapphire)晶体的常温力学性能.采用泡生法技术生长了尺寸为?180×280 mm3质量为30 kg的Fe, Ti: Sapphire晶体.实验发现,在蓝宝石晶体中掺入Fe2O3和TiO2以及相应的热处理可以显著提高晶体常温断裂强度、表面硬度和断裂韧性,而不损害晶体的可见和近红外透过性能;掺入的Fe2O3其Fe3+对Al3+的取代作用导致晶体内应力的增加,掺入的TiO2其Ti4+热处理时结晶出的第二相针状晶体的韧化效应,均对Fe, Ti: Sapphire晶体的力学性能的提高具有重要作用.研究对我国实现高强蓝宝石晶体应用材料具有重要现实意义.
@@@@Mechanical properties of titanium and iron co-doped Sapphire crystal are first studied at room temperature Large (?180 × 280 mm3 in dimension 30 kg in weight) titanium and iron codoped sapphire single crystal is grown by the Kyropoulos technique It is shown that the fracture strength and surface hardness and fracture toughness of as-grown crystals are significantly improved and the visible-infrared optical property is not adversely affected by titanium and iron codoping and certain heat treatment. The Fe3+ in the doped Fe2O3 palys a role of substituting Al3+, leading to an in creased internal stress in the crystal. And the Ti4+ in the doped TiO2 crystallizes the second phase needle crystal and brings in a toughening effect through certain heat treatment. As a consequence, the mechanical properties of as-grown sapphire are improved at room temperature. The present work has the realistic significance for developing the sapphires of excellent mechanical properties.

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以四丙基氢氧化铵(TPAOH)为模板剂,正硅酸乙酯(TEOS)为硅源,钛酸四丁酯(TBOT)为钛源,采用水热合成结晶法在堇青石载体上结晶生长TS-1晶体.实验考察了在175,℃、结晶时间3,d的条件下,不同水与硅源比例(硅源质量分数)、模板剂质量分数对TS-1晶体在堇青石载体上生长及其粒径的影响;同时通过SEM、ATR-FTIR、XRD表征手段分析TS-1晶体颗粒在堇青石载体上生长机理.结果表明,TS-1合成前驱液中硅源和模板剂质量分数直接影响TS-1晶体在堇青石载体上结晶过程中的骨架胶团浓度和过饱和度,通过控制过饱和度可以调控堇青石载体上TS-1纳米晶体颗粒的大小.
Titanium silicalite-1(TS-1)membranes were prepared to grow on cordierite support under hydrothermal treat-ment,using TPAOH as template,TEOS as silicate source,and TBOT as titanium source. The effect of ratios of Si/H2O and concentrations of structure-directing agent(SDA) synthesized at 175,℃ for 72,h was studied throughout experiments. TS-1,nanocrystal growing on cordierite support was analyzed with scanning electron microscope(SEM),X-ray diffractome-ter(XRD)and ATR-FTIR. The result indicates that the mechanism of TS-1,growth on cordierite support is that the concentra-tion of skeleton micelle and supersaturation of TS-1 precursor in the process of hydrothermal crystallization directly control the growth of TS-1 nanocrystal on the cordierite support.

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