目的比较并分析SYSMEX UF1000i全自动尿沉渣分析仪、Arkray AX-4030尿干化学分析仪及光学显微镜检测尿液红细胞的一致性。方法随机抽取427例患者新鲜尿液标本,分别用SYSMEX UF1000i全自动尿沉渣分析仪、Arkray AX-4030尿干化学分析仪及OLUMPUS光学显微镜进行检测,比较分析3种检测方法检测尿液红细胞的结果是否一致。结果以显微镜检查作为对照,SYSMEX UF1000i全自动尿沉渣分析仪对红细胞检测的敏感度、特异性为82.84%和86.35%,Arkray AX-4030尿干化学分析仪对红细胞检测的敏感度、特异性分别为89.55%和83.96%,SYSMEX UF1000i全自动尿沉渣分析仪对红细胞检测结果的Kappa值为0.580,一致性高;Arkray AX-4030尿干化学分析仪对红细胞检测结果的Kappa值为0.625,一致性高,SYSMEX UF1000i全自动尿沉渣分析仪与Arkray AX-4030尿干化学分析仪对红细胞检测结果的Kappa值为0.324,一致性较弱。结论将SYSMEX UF1000i全自动尿沉渣分析仪、Arkray AX-4030尿干化学分析仪作为过筛试验需结合光学显微镜检查进行复检,才能快速、准确地为临床提供有效、可靠的检验结果。

Objective To analyze the consistency of the SYSMEX UF1000i automatic urinary sediment analyzer,Arkray AX-4030 urine dry chemistry analyzer and optical microscope in detecting urine erythrocyte.Methods The fresh urine specimens from 427 patients were randomly extracted and tested by the SYSMEX UF1000i automatic urinary sediment analyzer,urine dry chemistry analyzer and OLUMPUS Arkray AX-4030 optical microscope.Then the consistency of the results for detecting urine erythrocyte was compared among three kinds of detection method.Results With the microscopic examination as control,the sensitivity and spe-cificity of the SYSMEX UF1000i automatic urinary sediment analyzer for detecting urine erythrocyte were 82.84% and 86.35% re-spectively,which of the Arkray AX-4030 urine dry chemistry analyzer were 89.55% and 83.96% respectively.There was a high consistency between the SYSMEX UF1000i automatic urinary sediment analyzer and the optical microscope for detecting urine e-rythrocyte a

目的：对贝克曼IMMAGE800免疫化学分析仪测定风湿三项（抗链球菌溶血素O(ASO)、类风湿因子（RF）、C反应蛋白（CRP））血清指标进行初步评价。方法：通过速率散射比浊法对ASO、RF、CRP血清指标的精密度、正确度、线性、携带污染等指标进行检测，评价贝克曼IMMAGE800免疫化学分析仪检测系统的性能。结果：IMMAGE800免疫化学分析仪的批内精密度（低水平）ASO变异系数（CV）为5.97%，RF和CRP的标准差（SD）分别为2.324、0.411，批内精密度（高水平）变异系数（CV）分别为3.43%、2.29%、4.54%，批间精密度（低水平）变异系数(CV)分别为4.46%、4.48%、4.81%，批间精密度（高水平）变异系数(CV)分别为5.09%、4.97%、3.35%。ASO、RF、CRP检测的相对偏差均小于CLIA’88或PT能力验证允许误差的1/2。ASO、RF、CRP检测的线性回归系数（r2）分别为0.9773、0.9939、0.9982。CRP携带污染率为-0.0193%。结论：IMMAGE800免疫化学分析仪具有良好的精密度、正确度、重复性和线性、携带污染率小,符合要求。

Objective:To evaluate the method for ASO,RF,CRP detection with IMMAGE800 Immune chemical analyzer.Methods:Though the method of rate scattering turbidimetry to detect the precision, accuracy, linear, carry pollution index for ASO,RF,CRP,and to evaluate the method for ASO,RF,CRP detection with IMMAGE800 Immune chemical analyzer.Result:The intra assay coefficient of variation(CV) of ASO of low value was 5.97%, and the standard deviation (SD) of RF and CRP were 2.324,0.411. The intra assay coefficient of variation(CV) of high value were 3.43%,2.29%,4.54%. The inter assay coefficient of variation(CV) of low and high value were 4.46%,4.48%,4.81%,5.09%,4.97%,3.35%. The relative deviation was less than half of the permissible error,which CLIA 88 or PT were allowed. The linear regression coefficient (r2) were 0.9773, 0.9939, 0.9982, respectively.The carry pollution rate of CRP was -0.0193%. Conclusion:The IMMAGE800 Immune chemical analyzer has good precision, accuracy, linear and carr

目的比较ROCHE URYSIS-2400尿液干化学分析仪(简称URYSIS-2400)和AIKELAI AX-4030尿液干化学分析仪(简称AX-4030)的检测结果的一致性。方法分别用URYSIS-2400和AX-4030平行测定500例尿液常规标本,比较检测结果的阳性检出率和符合率。随机选取250例使用尿沉渣显微镜复核尿红细胞(ERY)和白细胞(LEU)。通过添加实验评估URYSIS-2400、AX-4030抗维生素C干扰的能力。结果 2台仪器比重(SG)差异百分率均值1%,其余9项干化学检测项目一般符合率都90%。URYSIS-2400和AX-4030 ERY项目与尿沉渣显微镜计数的符合率分别为82.4%、84.4%,LEU分别为76.0%和83.2%。URYSIS-2400、AX-4030葡萄糖(GLU)和ERY项目添加维生素C浓度达50 mg/dL时不受干扰。结论 URYSIS-2400和AX-4030检测结果一致性良好,但尿液干化学分析仪只是筛检仪器,还应结合显微镜尿沉渣计数复核的结果以满足临床需要。

Objective To compare the consistency of ROCHE URYSIS-2400 and AIKELAI AX-4030 urine dry-chemistry analyzers.Methods A total of 500 urine specimens were detected by the 2 kinds of urine chemistry analyzers in parallel,and the results were analyzed statistically by positive detection rates and accordance rates.A total of 250 cases were randomly selected for reviewing erythrocytes (ERY)and leulcocytes (LEU)by urine sediment microscopy. Experiments by adding vitamin C were used to evaluate URYSIS-2400 and AX-4030 anti-interference abilities against vitamin C.Results The mean difference percentage of specific gravity (SG)between the 2 analyzers was 90%.The consistency rates of URYSIS-2400 and AX-4030 were 82.4% and 84.4% with urine sediment microscopy on ERY,and 76.0% and 83.2% on LEU. URYSIS-2400 and AX-4030 anti-interference abilities against vitamin C were up to 50mg/dL on glucose (GLU)and ERY.Conclusions There is a good consistency between the results of URYSIS-2400 and AX-4030,but urin

目的：研究对比临床尿常规不同检验方法的运用价值。方法搜集2013年9月～2014年9月我院接收的行尿常规检验38例患者，按照检验方法不同分为两组，即研究组（尿干化学分析仪）与对照组（手工镜检）。观察并比较研究组与对照组的检验结果。结果研究组红细胞检验阳性率高于对照组，白细胞阳性率和蛋白质阳性率均低于对照组，两组蛋白质检验结果符合率是98.3%，红细胞是97.0%，白细胞是96.6%，结果有统计学意义（P<0.05）。结论尿干化学分析仪与手工镜检在临床尿常规检验中均具有较高运用价值，但二者不可互相代替。

Objective The application value of different sampling methods in urine routine test is to be analyzed comparatively. Methods Choose 38 persons who took urine routine test in hospital from September 2013 to September 2014 and separate them into control group (urine dry chemistry analyzer) and study group (manual microscopic examination) according to different blood-sampling methods. And then observe and compare the testing results of two groups. Results Positive rate of red blood cel in study group is much higher than that in control group; however, the positive rate of leukocyte and protein in study group are much lower than counterparts in control group, the testing accuracy rate of protein content is 98.3%, it is 97.0%in testing accuracy rate of red blood cel and 96.6%in testing accuracy rate of leukocyte;such a result has statistic value(P<0.05);there is a treatment differential between the two groups, such a differential has statistic value(P<0.05). Conclusion Urine dry c

采用红外碳硫仪测定耐火材料中碳化硅的含量,选用多元助熔剂(LHDY01),缩短了操作时间,测定结果的相对标准偏差小于1.0%(n=8)。用该方法对两种碳化硅耐火材料样品进行测定,测定结果分别为16.16%,15.64%,与化学法测定结果 (15.99%,15.38%)相符合。该方法的精确度满足化学分析要求。

The silicon content of refractories containing silicon-carbide was determined by infrared carbon-sulfur analyzer. Multiple fulx (LHDY01) was used to shorten the operation time and reduce the analysis error. The relative standard deviation of determination results was less than 1.0%(n=8). Two samples were detected by this method, the results were 16.16%,15.64%, which were consistent with those (15.99%,15.38%) detected by chemical method. Precision and accuracy of the method can meet the requirement of chemical analysis.